Title :
Transmission EELS attachment for SEM
Author :
Luo, Tao ; Khursheed, Anjam
Author_Institution :
Centre for Integrated Circuit Failure Anal. & Reliability, Nat. Univ. of Singapore
fDate :
6/1/2006 12:00:00 AM
Abstract :
At the present transmission, an electron energy-loss spectrum (EELS) analysis is only carried out in transmission electron microscopes, such as the transmission electron microscopes (TEMs) or the Scanning Transmission Electron Microscopes (STEMs). Although the elemental analysis can be done in the scanning electron microscopes (SEMs) with an energy dispersive X-ray (EDX), its energy resolution is typically limited between 100-150 eV, nearly two orders of the magnitude larger than the energy resolution of the EELS in the TEMs/STEMs. This paper presents an EELS attachment for the conventional SEMs. K edge and the EELS low-loss spectrum of a thin amorphous carbon film are obtained in a Philips XL30 field emission SEM. The EELS attachment has the capability of acquiring structural information and 4 eV energy resolution at 30-keV primary beam energy
Keywords :
X-ray chemical analysis; X-ray spectroscopy; electron energy loss spectra; scanning electron microscopy; transmission electron microscopy; 100 to 150 eV; 30 keV; 4 eV; Philips XL30 field emission; aberration correction; carbon film; elemental analysis; energy dispersive X-ray; energy resolution; primary beam energy; scanning electron microscopes; scanning transmission electron microscopes; spectrometer; transmission electron energy-loss spectrum; Amorphous materials; Dispersion; Electron beams; Energy resolution; Filters; Magnetic separation; Scanning electron microscopy; Spectroscopy; Transmission electron microscopy; X-ray scattering; Aberration correction; EELS spectrum; energy resolution; spectrometer;
Journal_Title :
Device and Materials Reliability, IEEE Transactions on
DOI :
10.1109/TDMR.2006.876582