• DocumentCode
    1155200
  • Title

    A low-temperature ac microcalorimeter

  • Author

    Minakov, Alexander A.

  • Author_Institution
    Gen. Phys. Inst., Moscow, Russia
  • Volume
    30
  • Issue
    2
  • fYear
    1994
  • fDate
    3/1/1994 12:00:00 AM
  • Firstpage
    1058
  • Lastpage
    1060
  • Abstract
    The requirements for a low temperature ac microcalorimeter for heat-capacity and thermal-diffusivity measurements of microsamples weighted about 1 mg are considered. The influence of the wire-heat-leakage on the measured temperature oscillations is discussed. It is shown that the influence can lead to incorrect measurements. A proper choice of materials and external parameters enables the construction of a calorimeter with high sensitivity of about 10-8 J/K at 5 K. The presented calorimeter gives an opportunity to measure the heat capacity dependencies in the steady-state mode with a resolution ~0.01 K
  • Keywords
    calorimeters; calorimetry; specific heat of solids; thermal diffusivity; heat-capacity; low-temperature AC microcalorimeter; temperature oscillations; thermal-diffusivity; wire heat leakage; Building materials; Calorimetry; Heat transfer; Physics; Steady-state; Temperature measurement; Thermal conductivity; Weight measurement; Welding; Wires;
  • fLanguage
    English
  • Journal_Title
    Magnetics, IEEE Transactions on
  • Publisher
    ieee
  • ISSN
    0018-9464
  • Type

    jour

  • DOI
    10.1109/20.312493
  • Filename
    312493