Title :
Green synthesis of CdSe nanoparticles at room temperature and its characterisation
Author :
Sivasankar, K. ; Padmavathy, Nagarajan
Author_Institution :
Mater. Div., VIT Univ., Vellore, India
fDate :
3/1/2011 12:00:00 AM
Abstract :
L-Cysteine stabilised semiconductor CdSe nanoparticles were synthesised in aqueous medium by simple greener wet chemical method at room temperature from CdCl2.21/2H2O and Na2SeO3.5H2O and elemental selenium precursors for a short duration. The synthesised CdSe nanoparticles were characterised by powder X-ray diffraction (XRD), Fourier transform infrared (FTIR), UV-visible, transmission electron microscopy (TEM) and selected area electron diffraction (SAED) techniques. The powder XRD pattern and SAED pattern were in good agreement with each other and conform to the formation of single-phase CdSe nanoparticles. The FTIR studies reveal the capping effect of L-Cysteine in the formation of CdSe nanoparticles. The absorption maxima in UV-visible spectra clearly indicate the size quantisation effect and TEM image reveals that the size of the CdSe is about 10 nm.
Keywords :
Fourier transform spectra; II-VI semiconductors; X-ray diffraction; cadmium compounds; electron diffraction; infrared spectra; nanofabrication; nanoparticles; semiconductor growth; transmission electron microscopy; ultraviolet spectra; visible spectra; wide band gap semiconductors; CdSe; FTIR; Fourier transform infrared spectra; L-cysteine stabilised semiconductor nanoparticles; SAED; TEM; UV-visible spectra; XRD; green synthesis; powder X-ray diffraction; selected area electron diffraction; temperature 293 K to 298 K; transmission electron microscopy; wet chemical method;
Journal_Title :
Micro & Nano Letters, IET
DOI :
10.1049/mnl.2010.0201