Synthesis of Ni/TiO2 nanocomposite by loading TiO2 nanotubes with Ni nanoparticles

Synthesis of Ni nanoparticles on TiO₂ nanotubes was carried out using a pulsed electrodeposition technique. TiO₂ nanotubes were fabricated by anodization. The influence of the pulse electrodeposition conditions (current amplitudes, pulse time of negative current and substrate conductivity) was investigated on the surface morphology of Ni electrodeposited on TiO₂ nanotube arrays. The particle size and surface morphology of Ni deposits were studied by field emission scanning electron microscopy (FESEM). The result indicated that the average size of Ni nanoparticles was varied from 20 to 43 nm. The phase structure of Ni/TiO₂ materials was studied by X-ray diffraction (XRD). The experiment found that enhancing the conductivity of the TiO₂ nanotubes was a key factor for the successful deposition of Ni nanoparticles.