Title :
SnS nanostructures prepared by simple film technique: catalyst-free vacuum thermal evaporation
Author :
Jin Li ; Shengfeng Wang ; Jikang Jian ; Yanfei Sun ; Jinbao Xu
Author_Institution :
Key Lab. of Functional Mater. & Devices for Special Environments, Xinjiang Tech. Inst. of Phys. & Chem., Urumqi, China
Abstract :
SnS nanostructures were synthesised by simple vacuum thermal evaporation without any catalysts using tin chips and sulphur as the starting materials. The morphology was characterised by scanning electron microscopy and transmission electron microscopy (TEM) equipped with a high-resolution TEM. It was found that the as-prepared products were mostly tube shaped with a uniform geometry. The length of the nanostructures was several μm, the outer diameter and the thickness of the tubes was about 40-70 and 10-20 nm, respectively. The phase was analysed by X-ray diffraction and confirmed that the as-prepared products were of the orthorhombic phase. The photoluminescence spectra showed two emission bandcentres at 555.4 nm (2.24 eV) and at 785.0 nm (1.58 eV), which indicates that the SnS nanostructures could be used to prepare visible or an infrared light emitter or other optical devices.
Keywords :
X-ray diffraction; nanostructured materials; photoluminescence; scanning electron microscopy; tin compounds; transmission electron microscopy; vacuum deposition; SnS; X-ray diffraction; as-prepared products; catalyst-free vacuum thermal evaporation; electron volt energy 1.58 eV; electron volt energy 2.24 eV; emission bandcentres; high-resolution TEM; infrared light emitter; nanostructures; optical devices; orthorhombic phase; photoluminescence spectra; scanning electron microscopy; simple film technique; starting materials; tin chips; transmission electron microscopy; visible light emitter; wavelength 555.4 nm; wavelength 785 nm;
Journal_Title :
Micro & Nano Letters, IET
DOI :
10.1049/mnl.2013.0579