Title :
Biomimetic Synthesis of Calcium Phosphate Materials on Alkaline-Treated Titanium
Author :
Salemi, H. ; Behnamghader, A. ; Afshar, Ahmad ; Ardeshir, M. ; ForatiE, T.
Author_Institution :
Islamic Azad Univ. Sci. & Res. branch, Tehran
Abstract :
The hydroxyapatite coating on metal implants is a suitable method to create a bioactive surface and to increase the bone-implant bonding strength. In this research, at first the titanium surface was treated with NaOH solutions ; 5N and 10N at 60degC for 24 h and 5N at 60degC for 24 h followed by heating at 600degC for 1 h. The samples were immersed in the simulated body fluid (SBF) for 28 days to generate a calcium phosphate coating on titanium substrates. The modified substrates and coatings were characterized using SEM and XRD. According to the results obtained in this work the concentration increase of the NaOH solution has influenced the grain boundaries, whereas the heat treatment at 600degC has induced deeper and larger pores. Both the SEM images and the XRD spectra have illustrated the fact that the bone-like apatite had successfully been deposited on the titanium surface.
Keywords :
X-ray diffraction; biomedical materials; biomimetics; bone; calcium compounds; grain boundaries; prosthetics; scanning electron microscopy; sodium compounds; surface treatment; titanium; Ca3(PO4)2; NaOH; Ti; X-ray diffraction; alkaline treated titanium; bioactive surface; biomimetic synthesis; bone implant bonding strength; calcium phosphate materials; grain boundaries; metal implants; scanning electron microscopy; simulated body fluid; temperature 60 degC; temperature 600 degC; time 1 h; time 24 h; Biological materials; Biomimetics; Bonding; Calcium; Coatings; Heating; Implants; Surface treatment; Titanium; X-ray scattering; biomimetic; calcium phosphate; simulated body fluid; Alkalies; Biomimetic Materials; Biomimetics; Body Fluids; Bone Substitutes; Calcium Phosphates; Coated Materials, Biocompatible; Materials Testing; Sodium Hydroxide; Surface Properties; Titanium;
Conference_Titel :
Engineering in Medicine and Biology Society, 2007. EMBS 2007. 29th Annual International Conference of the IEEE
Conference_Location :
Lyon
Print_ISBN :
978-1-4244-0787-3
DOI :
10.1109/IEMBS.2007.4353679