Synthesis and Characterization of NH4V(Gly)3(PO4)2.H2O

Author

Wei, Bo ; Cao, Huiqun ; Sun, Jianmin ; Lv, Yujuan

Author_Institution

Chem. & Chem. Eng. Coll., Shenzhen Univ., Shenzhen, China

fYear

2009

fDate

11-13 June 2009

Firstpage

1

Lastpage

3

Abstract

A new vanadium-glycine complex (NH₄V(Gly)₃(PO₄)_2ldrH₂O) was synthesized in hydrothermal condition and characterized by XRD, FTIR, SEM and TG-DSC techniques. The results indicate that glycine and water exist in the crystal framework as ligand coordinating with vanadium. The SEM images show that the single crystals are homogeneous in crystal size and shape, and show a good crystalline performance. The size of crystals is about 20 times 20 times 20 mum³. It has a certain potential of application in studying the relationships between the chemical and biological properties of vanadium compounds.

Keywords

Fourier transform spectra; X-ray diffraction; crystal growth from solution; differential scanning calorimetry; infrared spectra; organic compounds; scanning electron microscopy; vanadium compounds; Fourier transform infrared spectra; X-ray diffraction; crystal shape; crystal size; dfferential scanning calorimetry; hydrothermal synthesis; scanning electron microscopy; thermal gravimetry; vanadium glycine complex; water; Amino acids; Chemistry; Crystallization; Fourier transforms; Infrared spectra; Powders; Scanning electron microscopy; Temperature; X-ray diffraction; X-ray scattering;

fLanguage

English

Publisher

ieee

Conference_Titel

Bioinformatics and Biomedical Engineering , 2009. ICBBE 2009. 3rd International Conference on

Conference_Location

Beijing

Print_ISBN

978-1-4244-2901-1

Electronic_ISBN

978-1-4244-2902-8

Type

conf

DOI

10.1109/ICBBE.2009.5163551

Filename

5163551