New method of synthesis of silver nanoparticles

Author

Pavlyukhina, L.A. ; Odegova, G.V. ; Kuzmina, S.L. ; Savintseva, S.A. ; Boldyrev, V.V.

Author_Institution

Inst. of Solid State Chem. & Mechanochem., Acad. of Sci., Novosibirsk, Russia

Volume

2

fYear

1999

fDate

1999

Firstpage

637

Abstract

Silver nanoparticles were prepared by reducing AgNO₃ with sodium hypophosphite in water-in-oil microemulsions in the presence of a mixture of ethoxylated alkylphenols as a surface-active substance (SAS). Ag/SAS/Al₂O₃ materials containing 0.04-0.13 wt% Ag were prepared by applying the microemulsions to an Al₂O₃ support and studied by diffuse reflection electronic spectroscopy, small-angle X-ray scattering, and X-ray diffraction. Ag particles in Ag/SAS/Al₂O₃ materials have a mean size of 70 W. The absorption band at 385 nm in the electronic spectra indicates that the nanoparticles consist of isolated clusters

Keywords

X-ray diffraction; nanostructured materials; silver; 385 nm; 70 A; Ag; Ag nanoparticles; AgNO₃; X-ray diffraction; diffuse reflection electronic spectroscopy; new method; small-angle X-ray scattering; synthesis; Chemistry; Hydrocarbons; Nanoparticles; Particle measurements; Petroleum; Reflection; Silver; Solid state circuits; Synthetic aperture sonar; Water;

fLanguage

English

Publisher

ieee

Conference_Titel

Science and Technology, 1999. KORUS '99. Proceedings. The Third Russian-Korean International Symposium on

Conference_Location

Novosibirsk

Print_ISBN

0-7803-5729-9

Type

conf

DOI

10.1109/KORUS.1999.876246

Filename

876246