Title :
Synthesization of carbon nanotubes using single stage thermal CVD method
Author :
Maryam, M. ; Suriani, A.B. ; Shamsudin, M.S. ; Rusop, M.
Author_Institution :
NANO-SciTech Centre, Univ. Teknol. MARA, Shah Alam, Malaysia
Abstract :
This paper will report on the synthesization of varieties of nanostructured carbon nanotubes such as bundles of vertically alligned CNTs (VACNTs), spaghetti-like CNTs and spiral-like structure of CNTs (SCNTs) which are potentially useful in various application. Multiwall carbon nanotubes (MWCNTs) were produced from palm oil precursor and ferrocene as catalyst source by this method at various deposition temperature ranging from 650-950°C with an increment of 50°C. Direct heat was used to vaporize both fixed parameter of precursor and catalyst placed in the middle of quartz tube. Field emission scanning electron microscopy was used to obtain the image of CNTs which showed different structures and diameters of CNTs relative to the deposition temperature of furnace. Raman Spectroscopy and Thermogravimetric analysis was also used to determine the purity of samples.
Keywords :
Raman spectroscopy; carbon nanotubes; catalysts; chemical vapour deposition; field emission electron microscopy; scanning electron microscopy; thermal analysis; Raman spectroscopy; VACNT; carbon nanotube synthesization; catalyst; direct heat; ferrocene; field emission scanning electron microscopy; furnace; multiwall carbon nanotube; nanostructured carbon nanotube; palm oil precursor; quartz tube; single stage thermal CVD method; spaghetti-like CNT; spiral-like structure; temperature 650 C to 950 C; thermogravimetric analysis; vertically alligned CNT; Carbon; Carbon nanotubes; Iron; Materials; Nanomaterials; Temperature distribution; carbon nanotubes; chemical vapor deposition; palm oil;
Conference_Titel :
Semiconductor Electronics (ICSE), 2012 10th IEEE International Conference on
Conference_Location :
Kuala Lumpur
Print_ISBN :
978-1-4673-2395-6
Electronic_ISBN :
978-1-4673-2394-9
DOI :
10.1109/SMElec.2012.6417110