Title :
Synthesis and characterization of copper oxides nanoparticles via pulsed laser ablation in liquid
Author :
Gondal, M.A. ; Qahtan, T.F. ; Dastageer, M.A. ; Saleh, T.A. ; Maganda, Y.W.
Author_Institution :
Phys. Dept., King Fahd Univ. of Pet. & Miner., Dhahran, Saudi Arabia
Abstract :
Pulsed laser ablation in liquids is a simple synthesis process of nano-particles for the production of high purity material with no need for any expensive instrumentation except laser. The 532 nm wavelength laser beam with 5 ns pulse width and 10 Hz repetition rate was an ablating laser source. In order to control the size and stoichiometry of the nano particles, the laser ablation was done in the presence of 9% of H2O2. The optical properties and structure of the prepared samples were studied using different analytical techniques, such as energy dispersive X-ray spectroscope (EDS), X-ray Diffraction, UV-Visible absorption, Photoluminescence, FT-IR. In order to study the morphology of the prepared nano-sized powders, Field Emission Scanning Electron Microscope was used. From the above analytical studies it was found that the particle size was between 13 and 28 nanometer, while the band gap energy was estimated to be 2.46 eV.
Keywords :
X-ray chemical analysis; X-ray diffraction; copper compounds; field emission electron microscopy; laser ablation; nanoparticles; particle size; photoluminescence; scanning electron microscopy; stoichiometry; CuO; EDS; FT-IR; UV-visible absorption; X-ray diffraction; ablating laser source; band gap energy; copper oxides nanoparticles; electron volt energy 2.46 eV; energy dispersive X-ray spectroscope; field emission scanning electron microscope; frequency 10 Hz; high purity material; laser beam; nanosized powders; optical properties; particle size; photoluminescence; pulsed laser ablation; size 13 nm to 28 nm; stoichiometry; time 5 ns; wavelength 532 nm; Chemical lasers; Copper; Laser ablation; Laser beams; Laser theory; Materials; Nanoparticles; Pulsed laser ablation; copper oxide; nanoparticles; optical;
Conference_Titel :
High Capacity Optical Networks and Enabling Technologies (HONET-CNS), 2013 10th International Conference on
Conference_Location :
Magosa
Print_ISBN :
978-1-4799-2568-1
DOI :
10.1109/HONET.2013.6729774