DocumentCode :
3506852
Title :
Characterization of TiO/sub 2/ films prepared by reactive magnetron sputtering at different oxygen partial pressures
Author :
Xu, L.X. ; Leng, Y.X. ; Yang, P. ; Zhang, Q. ; Gong, F.M. ; Huang, N.
Author_Institution :
Sch. of Mater. Sci. & Eng., Southwest Jiaotong Univ., Chengdu, China
fYear :
2004
fDate :
1-1 July 2004
Firstpage :
300
Abstract :
Summary form only given. The titanium oxide film is expected to be used as a coating for cardiovascular devices due to its excellent biocompatibility. Titania thin films were synthesized by the pulse unbalanced magnetron sputtering method. The effect of oxygen partial pressures on film properties has been studied. Titanium oxide films were deposited onto Ti/sub 6/Al/sub 4/V, glass and a silicon(100) wafer by DC reactive magnetron sputtering from a titanium metallic target with a purity of 99.9% in an Ar+O/sub 2/ gas mixture. Film structure and composition of the films were determined by X-ray diffraction (XRD) in a grazing angle configuration and X-ray photoelectron spectroscopy (XPS). The mechanical properties of the films were assessed by a ball-on-disk tribometer and Knoop micro-hardness tester, respectively. The light absorption behavior of films was measured by a UV755B spectrophotometer and the band gap of the films was calculated using the absorption curve. The sessile method of contact angle measurement was carried out on a JY-82 goniometer on sheet samples using eight kinds of liquids. The surface energy of the films was calculated using the contacting angle.
Keywords :
X-ray diffraction; X-ray photoelectron spectra; biomedical materials; contact angle; energy gap; hardness testing; microhardness; sputter deposition; sputtered coatings; stoichiometry; surface energy; thin films; titanium compounds; ultraviolet spectra; DC reactive magnetron sputtering; JY-82 goniometry; Knoop microhardness tester; Si; TiAlV; TiO/sub 2/; TiO/sub 2/ films; UV755B spectrophotometry; X-ray diffraction; X-ray photoelectron spectroscopy; XPS; XRD; ball on disk tribometry; band gap; biocompatibility; cardiovascular devices; contact angle; contacting angle; film composition; film structure; gas mixture; glass; light absorption; mechanical properties; oxygen partial pressure; pulse unbalanced magnetron sputtering; sessile method; silicon(100) wafer; surface energy; titania thin films; titanium metallic target; titanium oxide film; Cardiology; Coatings; Electromagnetic wave absorption; Glass; Goniometers; Semiconductor films; Sputtering; Titanium; X-ray diffraction; X-ray scattering;
fLanguage :
English
Publisher :
ieee
Conference_Titel :
Plasma Science, 2004. ICOPS 2004. IEEE Conference Record - Abstracts. The 31st IEEE International Conference on
Conference_Location :
Baltimore, MD, USA
ISSN :
0730-9244
Print_ISBN :
0-7803-8334-6
Type :
conf
DOI :
10.1109/PLASMA.2004.1339974
Filename :
1339974
Link To Document :
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