Title :
Research on fabrication of PQ:PMMA photopolymer
Author :
Lin, Shiuan-Huei ; Lin, June-Hua ; Hsu, Ken Y.
Author_Institution :
Inst. of Electrophys., Nat. Chiao Tung Univ., Hsinchu, Taiwan
Abstract :
The standard procedure to make PQ:PMMA samples with high optical quality is presented here. We add 0.7 wt.% of PQ (Phenanthrenequinone) and 1 wt.% of AIBN (Azobisisobutyronitrile) into the solvent MMA (Methyl methacrylate) to form the MMA solution. From our investigation, we found that the key that affects the material quality is the time of the second stir. During this period, the viscosity of the solution is increasing. In this paper, the Ubbelohde capillary is used to measure the relative viscosity of the MMA solution. The capillary set up which contains the solution or the solvent MMA solution is put in a water bath at 30 °C. In a linear approximation, the falling time is proportional to the viscosity of the liquid, which is in turn linearly proportional to its density.
Keywords :
capillarity; optical fabrication; optical polymers; viscosity measurement; 30 C; MMA solution viscosity; PQ:PMMA photopolymer fabrication; Ubbelohde capillary; azobisisobutyronitrile; high optical quality; linear approximation; material quality; methyl methacrylate; phenanthrenequinone; solvent MMA; Contracts; Councils; Density measurement; Equations; Fabrication; Linear approximation; Optical materials; Solvents; Time measurement; Viscosity;
Conference_Titel :
Lasers and Electro-Optics, 2003. CLEO/Pacific Rim 2003. The 5th Pacific Rim Conference on
Print_ISBN :
0-7803-7766-4
DOI :
10.1109/CLEOPR.2003.1274829