Title :
Properties of MgB2 films with very high transport critical current densities
Author :
Kitaguchi, Hitoshi ; Doi, Toshiya ; Kobayashi, Yuki ; Matsumoto, Akiyoshi ; Sosiati, Harini ; Hata, Satoshi ; Fukutomi, Masao ; Kumakura, Hiroaki
Author_Institution :
Oxide Supercond. Wires Group, Nat. Inst. for Mater. Sci., Tsukuba, Japan
fDate :
6/1/2005 12:00:00 AM
Abstract :
Magnesium diboride, MgB2, thin films are fabricated through two different kinds of process. One is an in-situ process by using electron beam deposition and the other is an ex-situ process by using the combination of pulsed laser deposition and heat treatment. The critical current density, Jc, is investigated as a function of external magnetic field in the range of 0-7 T and/or temperatures ranging from 4.2 K to the critical temperature by using dc 4-probe transport method. The in-situ processed film shows very high Jc, e.g., 7.1×106, 1.2×106, and 1.4×105 A/cm2 in 0, 4, and 7 T (perpendicular fields), respectively. Angular dependence of Jc is much different between the two kinds of films. Jc-angle (magnetic field) curves of the in-situ processed film show two peaks; one is around the field perpendicular to the film surface and the other is around the parallel field. On the contrary, the curves of the ex-situ processed film have only one peak around the parallel field. Microstructure analyses show that the in-situ film has columnar grains aligned perpendicular to the film surface and that the ex-situ one has granular grains with random orientations. These results indicate that the grain boundaries between columnar grains act as effective pinning centers and enhance Jc in the perpendicular fields.
Keywords :
critical current density (superconductivity); electron beam deposition; electron density; flux pinning; grain boundaries; heat treatment; magnesium compounds; magnetic flux; pulsed laser deposition; superconducting thin films; superconducting transition temperature; type II superconductors; 0 to 7 T; 4.2 K; MgB2; MgB2 films; angular dependence; columnar grains; dc 4-probe transport method; electron beam deposition; ex-situ process; grain boundary; granular grains; heat treatment; in-situ process; irreversibility fields; magnesium diboride; magnetic field; microstructure analyses; pinning centers; pulsed laser deposition; random orientations; thin films; transport critical current density; Critical current density; Electron beams; Heat treatment; Magnesium compounds; Magnetic fields; Magnetic films; Optical pulses; Pulsed laser deposition; Temperature distribution; Transistors; Critical current densities; irreversibility fields; pinning; thin films;
Journal_Title :
Applied Superconductivity, IEEE Transactions on
DOI :
10.1109/TASC.2005.848866