Title :
A Low-Power Pressure- and Temperature-Programmable Micro Gas Chromatography Column
Author :
Potkay, Joseph A. ; Lambertus, Gordon Randall ; Sacks, Richard D. ; Wise, Kensall D.
Author_Institution :
Louis Stokes Cleveland VA Med. Center, Cleveland
Abstract :
This paper presents the theory, fabrication, and experimental results for a high-performance low-power micro gas chromatography column. The suspended-dielectric 1-m-long column is split into two sections, permitting independent pressure and temperature programming. Integrated column heaters have a mean resistance of 16.8 kOmega and a temperature coefficient of resistance of 431 ppm/degC. The suspended column requires 11 mW to raise its temperature by 100degC in vacuum (1 mtorr). The column separates ten volatile organic compounds in 52 s and four chemical warfare agent simulants and an explosive simulant in 60 s.
Keywords :
chromatography; dielectric heating; micromachining; microsensors; transducers; chemical transducer; gas detector; high-performance low-power micro gas chromatography column; integrated column heaters; mean resistance; micromachining; power 11 mW; resistance 16.8 kohm; size 1 m; suspended-dielectric column; temperature coefficient of resistance; temperature programming; Biomedical engineering; Chemical industry; Fabrication; Gas chromatography; Immune system; Laboratories; Monitoring; Resistance heating; Temperature sensors; Volatile organic compounds; Chemical transducers; column; gas chromatography (GC); gas detectors; low power; micromachining;
Journal_Title :
Microelectromechanical Systems, Journal of
DOI :
10.1109/JMEMS.2007.902470