Title of article :
Preparation, crystal structure and thermal decomposition process of [Y(NTO)2 NO3(H2O)5]·2H2O
Author/Authors :
Song Jirong، نويسنده , , Ning Binke، نويسنده , , Hu Rongzu، نويسنده , , Kang Bin Wang، نويسنده ,
Issue Information :
دوهفته نامه با شماره پیاپی سال 2000
Pages :
5
From page :
111
To page :
115
Abstract :
[Y(NTO)2 NO3(H2O)5]·2H2O was prepared by mixing the aqueous solution of lithium 3-nitro-1,2,4-triazol-5-onate and the dilute nitric acid solution of yttrium oxide. The single crystal structure has been determined by a four-circle X-ray diffractometer. The crystal is monoclinic, space group Cm with crystal parameters of a=0.6773(2) nm, b=2.0866(2) nm, c=0.6551(1) nm, β=102.98(2)°, V=0.9021(1) nm, Z=2, Dc=1.970 g cm−3, μ=33.487 cm−1, F(000)=540. The final R is 0.032. Based on the thermal analysis, the thermal decomposition process of [Y(NTO)2 NO3(H2O)5]·2H2O has been derived.
Keywords :
Thermal decomposition process , Yttrium complex of NTO , Preparation , crystal structure
Journal title :
Thermochimica Acta
Serial Year :
2000
Journal title :
Thermochimica Acta
Record number :
1194686
Link To Document :
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