Title of article :
Synthesis of Ph2LSn(μ-OH)Bu3SnCl. Trapping of monomeric triorganotin hydroxide Ph2LSnOH
Author/Authors :
Libor Dost?l، نويسنده , , Jan Taraba، نويسنده , , Roman Jambor، نويسنده ,
Issue Information :
دوفصلنامه با شماره پیاپی سال 2009
Pages :
3
From page :
1251
To page :
1253
Abstract :
The reaction of triorganotin(IV) compound Ph2LSnCl (1), (L = 2,6-(t-BuOCH2)2C6H3), with (Bu3Sn)2O resulted to the isolation of Ph2LSn(μ-OH)Bu3SnCl (2), in which a monomeric triorganotin(IV) hydroxide Ph2LSnOH intermolecularly coordinates Bu3SnCl moiety. Compound 2 was characterized by combination of 1H, 13C and 119Sn NMR spectroscopy, ESI/MS, elemental analysis and X-ray diffraction.
Keywords :
NMR spectroscopy , crystal structure , Pincer ligands , Organotin compounds
Journal title :
Journal of Organometallic Chemistry
Serial Year :
2009
Journal title :
Journal of Organometallic Chemistry
Record number :
1376978
Link To Document :
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