Issue Information :
روزنامه با شماره پیاپی سال 2004
Pages :
5
From page :
521
To page :
525
Abstract :
This paper reports that Zn3N2 powder of high quality has been synthesized by a nitridation reaction of Zn powder with NH3 gas (flow rate 500 ml/min) at the nitridation temperature of 600 °C for 120 min. X-ray diffraction indicates that Zn3N2 is cubic in structure with the lattice constant being a=9.788 Å. X-ray photoelectron spectroscopy shows the differences of chemical bonding states between Zn3N2 and ZnO, and confirms the formation of N–Zn bonds. Thermal gravimetric analysis and differential thermal analysis are employed to investigate the thermal decomposition behavior of Zn3N2 powder. It is found that Zn3N2 is unstable when exposed to open air above 500 °C.
Journal title :
Acta Tropica
Serial Year :
2004
Journal title :
Acta Tropica
Record number :
1748767
Link To Document :
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