Title of article :
Synthesis and characterization of 6-(hydroxymethyl)-14,16-dimethyl-13,14,16,17-tetrahydro-6H-13,17-epiminodibenzo[e,-l][1,4]dioxacyclotridecin-15(7H)-one
Author/Authors :
Banaei ، Alireza - Payame Noor University , Karimi ، Soheyla - Payame Noor University , Nurbageri ، Negar - Payame Noor University
Abstract :
New 6-(hydroxymethyl)-14,16-dimethyl-13,14,16,17-tetrahydro-6H-13,17- epiminodibenzo[e,l][1,4]dioxacyclotridecin-15(7H)-one(2a) was synthesized in good yield by the Petrenko-Kritchenko reaction of 2,2 -((3-hydroxypropane-1,2-diyl)bis- (oxy))bisbenzaldehyde(1a) with diethyl ketone in the mixture of ethanol and acetic acid as solventin the presence of ammonium acetate. The compounds were characterized by elemental analyses, IR, 1H-NMR, 13C-NMR and mass spectrometry.
Keywords :
Petrenko , Kritchenko condensation , macrocyclic compound , bisaldehyde
Journal title :
Iranian Chemical Communication
Journal title :
Iranian Chemical Communication
