Title :
A tunable continuous-wave 330 GHz gyrotron for enhanced nuclear magnetic resonance
Author :
Torrezan, A.C. ; Shapiro, M.A. ; Sirigiri, J.R. ; Temkin, R.J.
Author_Institution :
Plasma Sci. & Fusion Center, MIT, Cambridge, MA, USA
Abstract :
Summary form only given. Dynamic nuclear polarization (DNP) is a technique used to enhance the signal-to-noise ratio in nuclear magnetic resonance (NMR) experiments and requires a continuous-wave (CW) source able to generate ten or more watts of power in the 140 to 600 GHz range, a task well suited for gyrotron oscillators. Besides these requirements, a frequency tunable gyrotron is also highly desirable since it would permit DNP/NMR experiments to be performed without tuning the NMR magnet or with NMR magnets without a superconducting sweep coil. We have performed preliminary tuning experiments in a CW 460 GHz gyrotron that have demonstrated 1 GHz of magnetic/voltage tuning at 460 GHz, second-harmonic mode TE11,2, with a maximum power of 16 W When the magnetic field was reduced, we also obtained at 332 GHz, second-harmonic mode TE4,3, a maximum power of 2.5 W with 1 GHz of tuning. We are now fabricating a CW 330 GHz gyrotron oscillator operating at the second harmonic of the cyclotron frequency that will be integrated to a 500 MHz DNP/NMR spectrometer. The gyrotron is designed to operate in the TE4,3 mode, with a 35-mm long cylindrical cavity, radius 1.83 mm. The mode interacts with a 9.5 kV, 100 mA electron beam, radius 1.08 mm, with perpendicular velocity spread of less than 5% and pitch factor of 1.8 according to EGUN simulations. The start oscillation current was computed to be as 32 mA. Self- consistent simulations using the code MAGY estimate a maximum output power of 60 W and a magnetic tuning range of 600 MHz by exciting high order axial modes. Extended tuning range is expected to be obtained by a thermal tuning scheme implemented in the tube. The generated radiation is coupled out of the gyrotron by means of a helical cut launcher and a series of mirrors.
Keywords :
NMR spectrometers; SCF calculations; dynamic nuclear polarisation; gyrotrons; harmonic generation; millimetre wave oscillators; tuning; DNP-NMR spectrometer; EGUN simulations; NMR magnets; code MAGY estimate; continuous-wave source; current 100 mA; cyclotron frequency; cylindrical cavity; dynamic nuclear polarization; enhanced nuclear magnetic resonance; frequency 1 GHz; frequency 330 GHz; frequency 332 GHz; frequency 460 GHz; frequency 500 MHz; frequency 600 MHz; frequency tunable gyrotron; gyrotron oscillators; helical cut launcher; high-order axial modes; magnetic-voltage tuning; mirrors; perpendicular velocity; pitch factor; power 16 W; power 2.5 W; power 60 W; second-harmonic mode TE11,2; second-harmonic mode TE4,3; self-consistent simulations; signal-to-noise ratio; size 1.08 mm; size 1.83 mm; size 35 mm; thermal tuning scheme; tunable continuous-wave gyrotron; voltage 9.5 kV; Computational modeling; Frequency; Gyrotrons; Nuclear magnetic resonance; Oscillators; Power generation; Superconducting coils; Superconducting magnets; Tellurium; Tuning;
Conference_Titel :
Plasma Science - Abstracts, 2009. ICOPS 2009. IEEE International Conference on
Conference_Location :
San Diego, CA
Print_ISBN :
978-1-4244-2617-1
DOI :
10.1109/PLASMA.2009.5227689