Title :
Copper nanoparticle synthesis in continuous mode by the polyol method - Progress towards Nanomanufacturing
Author :
Ramprasad, Sudhir ; Ramsing, Patrick E. ; Miller, R. Todd ; Rundel, Jack T. ; Remcho, Vincent T. ; Palo, Daniel R.
Author_Institution :
Pacific Northwest Nat. Lab., Corvallis, OR, USA
Abstract :
Transition of batchwise nanoparticle production routes to large-scale manufacturing processes is vital for commercialization of such materials. This paper reports the comparison studies from batch and continuous mode for the synthesis of copper nanoparticles by the polyol method. The copper nanoparticles synthesized in continuous mode utilizing a novel microchannel mixer were found to be comparable to the nanoparticles developed in batch mode. Transmission Electron Microscopy (TEM), X-Ray Diffraction (XRD), and Selected Area Electron Diffraction (SAED) techniques were used for characterization of the copper nanoparticles produced.
Keywords :
X-ray diffraction; copper; electron diffraction; manufacturing processes; nanoparticles; transmission electron microscopy; Cu; X-ray diffraction; batch mode; continuous mode; copper nanoparticle; large-scale manufacturing; microchannel mixer; nanomanufacturing; polyol method; selected area electron diffraction; transmission electron microscopy; Aging; Copper; FCC; Nanoparticles; Printing; X-ray diffraction; X-ray scattering;
Conference_Titel :
Nanotechnology (IEEE-NANO), 2011 11th IEEE Conference on
Conference_Location :
Portland, OR
Print_ISBN :
978-1-4577-1514-3
Electronic_ISBN :
1944-9399
DOI :
10.1109/NANO.2011.6144341