Title :
Characterization of green synthesized copper nanoparticles: A novel approach
Author :
Suresh, Y. ; Annapurna, S. ; Bhikshamaiah, G. ; Singh, A.K.
Author_Institution :
Dept. of Phys., Osmania Univ., Hyderabad, India
Abstract :
Green synthesis of metal nanoparticles is considered to be a cost effective and eco-friendly approach. In the present study copper nanoparticles were synthesized successfully through chemical reduction of different copper salts stabilized by potato starch. The resulting copper nanoparticles were characterized by X-Ray Diffraction (XRD) spectrum, Fourier Transform Infrared (FTIR) Spectroscopy, Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM) to study the size and shape of the particles and functional group of the stabilizing agent. The particle sizes are found to be in the range of 5 to 40 nm with FCC structure of copper nanoparticles. The rate of formation of copper nanoparticles was studied by using UV Visible Absorption Spectroscopy by measuring the absorbance at around 554 nm. The Surface Enhanced Raman Spectroscopy (SERS) results showed the formation of copper nanoparticles.
Keywords :
Fourier transform spectra; X-ray diffraction; copper; infrared spectra; nanofabrication; nanoparticles; particle size; reduction (chemical); scanning electron microscopy; surface enhanced Raman scattering; transmission electron microscopy; ultraviolet spectra; visible spectra; Cu; FCC structure; FTIR; Fourier transform infrared spectroscopy; SEM; SERS; TEM; UV visible absorption spectroscopy; X-ray diffraction; XRD spectrum; chemical reduction; copper nanoparticle formation rate; copper salts; functional group; green synthesis; green synthesized copper nanoparticle characterization; metal nanoparticles; particle shape; particle size; potato starch; scanning electron microscopy; size 5 nm to 40 nm; stabilizing agent; surface enhanced Raman spectroscopy; transmission electron microscopy; Copper; X-ray scattering; Green synthesis; SERS; copper nanoparticles; potato starch;
Conference_Titel :
Advanced Nanomaterials and Emerging Engineering Technologies (ICANMEET), 2013 International Conference on
Conference_Location :
Chennai
Print_ISBN :
978-1-4799-1377-0
DOI :
10.1109/ICANMEET.2013.6609236